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Laboratory of Supercritical Fluid Extraction Process Engineering (LSFEPE) - UPB
University POLITEHNICA of Bucharest
Short link:
https://eeris.eu/
ERIF-2000-000A-5377
128
Visits
Research areas of laboratory involve: - extraction of pigments, volatile oils, vegetable oils and other valuable compounds from seeds, medicinal herbs, food and agricultural waste - kinetics of supercritical extraction process - optimal extraction conditions for achieving high yields of target compounds - modelling, simulation and optimization of supercritical extraction processes - scale-up of supercritical extraction processes - high pressure measurements of liquid-supercritical fluid sy...
Petrica
IANCU
p_iancu@chim.upb.ro
Associate Professor
SCIENTIFIC TEAM
8
Costin Sorin BILDEA
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Valentin CROITORU
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Adrian GORA
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Ion LEMNARU
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Valentin PLESU
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Mihaela POPESCU
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Nicoleta-Gabriela STEFAN
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Elena Catalina UDREA
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Pilot Plants for Process Testing, Chemical and biochemical process engineering, Food Science and Engineering
RI Domain of activity
Research Data Management Plan:
No information available
Access Policy to Research Infrastructure and Related Services:
No information available
Research Services
Supercritical fluid extraction of bioactive compounds from solid plant matrices
SERVICE DESCRIPTION:
SERVICE PERSONS:
Valentin PLESU
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Costin Sorin BILDEA
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Mihaela POPESCU
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Adrian GORA
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Ion LEMNARU
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Valentin CROITORU
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Supercritical fluid extraction of bioactive compounds from vegetal liquids
SERVICE DESCRIPTION:
SERVICE PERSONS:
Valentin PLESU
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Costin Sorin BILDEA
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Mihaela POPESCU
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Adrian GORA
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Valorisation of bioresources and wastes
SERVICE DESCRIPTION:
SERVICE PERSONS:
Valentin PLESU
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Mihaela POPESCU
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Nicoleta-Gabriela STEFAN
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Quantitative and qualitative analysis of bioactive compounds from plant extracts
SERVICE DESCRIPTION:
SERVICE PERSONS:
Mihaela POPESCU
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Nicoleta-Gabriela STEFAN
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High pressure thermodynamic properties
SERVICE DESCRIPTION:
SERVICE PERSONS:
Valentin PLESU
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Mihaela POPESCU
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Elena Catalina UDREA
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Modelling, simulation, optimisation, scale-up of extraction processes
SERVICE DESCRIPTION:
SERVICE PERSONS:
Valentin PLESU
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Mihaela POPESCU
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Elena Catalina UDREA
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Research Equipment
Supercritical liquid/solid extraction plant HPE-CC 500
CATALOG NAME:
HPE-CC 500, Ser. No. 427, 435, 436a,b,c
DESCRIPTION:
The high pressure extraction unit HPE-CC 500 is a multipurpose system for research and development. It is designed to study either solid extraction or counter-current extraction of harmless liquid feeds by use of supercritical carbon dioxide (CO2). The equipment is divided into three sections: 1. Section A for extraction of a liquid in a high-pressure counter-current column. The extraction column has Sulzer CY type packing, a capacity of 3.9 L and an internal diameter of 38 mm. The operating limits in this section are the extraction temperature of 100 ºC and the extraction pressure of 300 bar. 2. Section B for solid extraction. The extraction vessel has a capacity of 3.2 L. The operating limits in this section are the extraction temperature of 120 ºC and the extraction pressure of 500 bar. 3. Section C for liquid – gas separation. The separation vessel has a capacity of 1.2 L The operating limits in this section are the temperature of 80 ºC and the pressure of 150 bar. This unit allows the use of liquid and solid plant materials for isolation and recovery of target compounds with high biological and economic value.
PRODUCER:
EUROTECHNICA GmbH, Germany
PRODUCTION YEAR:
2019
COMMISSIONING DATE:
PRICE RANGE (at the time of purchase)
DATA SHEET:
High pressure viscosimeter HP – vis500
CATALOG NAME:
HP – vis500, Ser. No. 430
DESCRIPTION:
The high pressure viscometer HP-vis500 is designed for viscosity measurements at elevated pressures and temperatures. Gases and liquids may be used and saturated/mixed in a movable piston accumulator. An automatic syringe pump is used to create a constant flow of the fluid. The pressure is regulated and released by a manual back pressure regulating system with a buffer vessel using a compressible fluid e.g. nitrogen. The viscosity range of the capillary tubes is between 0.1-100 mPa•s. The pressure difference is measured between the in- and outlet of a capillary tube coil enabling the determination of the viscosity. The operating limits in this equipment are the temperature of 150 °C and the pressure of 500 bar.
PRODUCER:
EUROTECHNICA GmbH, Germany
PRODUCTION YEAR:
2019
COMMISSIONING DATE:
PRICE RANGE (at the time of purchase)
DATA SHEET:
High pressure view chamber coupled with mini dosing device HPVC – 500v
CATALOG NAME:
HPVC – 500v, Ser. No. 429
DESCRIPTION:
The high pressure view vhamber HPVC – 500v is designed for observation of phase behaviour and reactions at elevated temperatures and pressures, to measure the interfacial tension of a liquid in the fluid medium and the contact angle of a liquid on a chosen material. Phase equilibrium measurements involve observing the behavior of a liquid phase in the fluid atmosphere. Inter-facial tension measurements involve the distribution of a drop of liquid in a fluid medium. The contact angle measurements involve the distribution of a drop of a liquid on a material, in a fluid medium. The operating limits in this equipment are the temperature of 150 °C and the pressure of 500 bar.
PRODUCER:
EUROTECHNICA GmbH, Germany
PRODUCTION YEAR:
2019
COMMISSIONING DATE:
PRICE RANGE (at the time of purchase)
DATA SHEET:
FT-IR spectrometer
CATALOG NAME:
VERTEX 70
DESCRIPTION:
FT-IR spectrometer is used to analyze plant extracts from the qualitative and quantitative point of view. The equipment has a transmission device (T) and an attenuated total reflection device (ATR) which allows a rapid analysis of plant extracts without further preparation.
PRODUCER:
Bruker
PRODUCTION YEAR:
2018
COMMISSIONING DATE:
PRICE RANGE (at the time of purchase)
DATA SHEET:
Soxhlet extraction system
CATALOG NAME:
DESCRIPTION:
The Soxhlet extraction system consist in two interconnected batteries with extractors of 250 mL and spare parts for extractors, condenser and extract vessels. This system is used for the conventional extraction of target compounds from solid plant matrices.
PRODUCER:
ISOLAB
PRODUCTION YEAR:
2018
COMMISSIONING DATE:
PRICE RANGE (at the time of purchase)
DATA SHEET:
Rotavapor
CATALOG NAME:
DESCRIPTION:
The rotavapor is used to evaporate the solvent from the plant material extracts resulted from the conventional extraction methods. The capacity of the solvent collector vessel is 500 mL.
PRODUCER:
PRODUCTION YEAR:
2000
COMMISSIONING DATE:
PRICE RANGE (at the time of purchase)
DATA SHEET:
Laboratory oven
CATALOG NAME:
DESCRIPTION:
The laboratory oven is used to dry the plant materials used in the extraction processes. The equipment has three trays, an independent overheat thermostat and the temperature range is between 40-250 °C.
PRODUCER:
GenLab
PRODUCTION YEAR:
2010
COMMISSIONING DATE:
PRICE RANGE (at the time of purchase)
DATA SHEET:
Phone:
+ 4021-402 9216
Fax:
+4021-3185900
Gheorghe Polizu
,
1, Building R, Room R020
,
Bucuresti
011061
,
Bucuresti - Sector 1
Romania
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[T: 0.6908, O: 392]
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